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Title: | 超高真空TEM-AFMを用いた清浄な原子スケール金属接点力学特性の解明 |
Other Titles: | A study of mechanical property of clean metal atomic contacts by UHV-TEM-AFM method |
Authors: | 大島, 義文 |
Authors(alternative): | Oshima, Yoshifumi |
Keywords: | 透過型電子顕微鏡 水晶振動子 金属ナノ接点 力学的性質 |
Issue Date: | 1-Jun-2018 |
Abstract: | 水晶振動子の共振周波数シフトを用いた力計測を組み込んだTEM-AFMホルダーを設計・開発し、金ナノ接点のヤング率について直径依存性を明らかにした。この力計測法は、水晶振動子の高い共振周波数、および、高いバネ定数を活用することで、極めて小さな振幅でも原子スケールの力の傾きを計測できた。信号ノイズの対策を行うことで、約6N/mの分解能で力の傾き(つまり、等価バネ定数)を計測できる。また、振動子の振幅が約80pmと小さいため、力計測と同時に原子分解能像を得ることも可能であった。解析より、金ナノ接点のヤング率は、直径10nm以下になると徐々に低下することを定量的に明らかに出来た。:We designed and developed TEM-AFM holder, which can measure atomic-scale force using resonance frequency shift of quartz crystal resonator in order to clarify thedependence on Young's modulus of gold nano-contact. In this force measurement method, by utilizing the high resonance frequency and the high spring constant of the quartz resonator, it is possible to measure the atomic scale force gradient even with extremely small amplitude of the resonator. Byreducing signal noise, it is possible to measure the force gradient (that is, the equivalent spring constant) with a resolution of about 6 N/m. In addition, since the amplitude of the oscillator is as small as about 80 pm, it is possible to acquire atomic resolution image simultaneously with force measurement. From the analysis, it is possible to quantitatively clarify that the Young's modulus of the gold nano-contact gradually decreases as the diameter becomes 10 nm or less. |
Description: | 基盤研究(B)(一般) 研究期間:2015~2017 課題番号:15H03522 研究者番号:80272699 研究分野:表面物性 |
Language: | jpn |
URI: | http://hdl.handle.net/10119/15397 |
Appears in Collections: | 2017年度 (FY 2017)
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15H03522seika.pdf | | 324Kb | Adobe PDF | View/Open |
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